MARK WILLETTE
Senior Laboratory Technician at CMC Materials- Claim this Profile
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Bio
Experience
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CMC Materials
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United States
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Semiconductor Manufacturing
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200 - 300 Employee
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Senior Laboratory Technician
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Dec 2021 - Present
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WM
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United States
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Environmental Services
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700 & Above Employee
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Laboratory Manager
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Jun 2017 - May 2022
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McCampbell Analytical, Inc.
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United States
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Environmental Services
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1 - 100 Employee
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Volatiles Group Supervisor / Chemist
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Jul 2015 - Nov 2016
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SGS Galson
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United States
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Environmental Services
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1 - 100 Employee
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GC/MS Section Supervisor
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Sep 2013 - Jul 2015
RESPONSIBILITIES Personnel decisions in the TO-15 / T0-17 group including hiring, firing, disciplinary actions, and performance evaluations. Verifying accuracy and completeness of all results and data packages generated by department including Level four deliverables. Training and coaching of all analysts in the department. This includes teaching GC/MS trouble shooting skills, Entech optimization, computer skills, chromatography skills, and Standard Operating Procedures. Interface with other departments, especially QA and the IT departments to increase quality and efficiency. ACCOMPLISHMENTS Increased the efficiency of the GC/MS department through optimization of the Entech autosamplers and preconcentrators. Instituted a culture of continuous improvement within the department, through meetings and brainstorming sessions. Improved multiple aspects of routine operations using skills and knowledge gained at previous positions. Show less
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M. A. Silva USA
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Santa Rosa, CA
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GC/MS expert
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Apr 2013 - Jun 2013
Short term contract) RESPONSIBIILITIES Evaluate initial status of GC/MS system, and bring back to operational status Learn software and hardware Of the GC/MS system Develop and validate a method for target compound analysis Write detailed operating procedure and train staff on the procedure ACCOMPLISHMENTS Optimized analytical parameters to meet stringent (low) method reporting limits and a to make analysis more robust Wrote detailed Standard Operating Procedure detailing procedure step-wise so the document can be used for training future staff members Trained department manager on procedure, including Mass Spectral theory, calibration theory and troubleshooting of the application Show less
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Scientist
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Apr 2010 - Oct 2012
RESPONSIBILITIES Assuring Turnaround times and quality objectives are met for all analyses. Coaching, training and mentoring analysts in analytical techniques, efficiency and quality goals. Scheduling samples and workload for the VOC department. Maintaining stock and working standard materials inventory. Working with quality assurance and customer service departments to ensure quality, timely data is generated and customer expectations are met. Assisting with all outside audits of the VOC department. Data reduction, review and reporting. ACCOMPLISHMENTS Helped department to achieve and maintain a sub 5 day turnaround time and to decrease the Summa canister turnaround time, maximizing the usefulness of the existing canister inventory through coaching and training of new and existing staff members. Led a project to increase throughput by use of auto-samplers and dual trap techniques for analyzing air samples, resulting in 24 hour operations without the use of 3 shifts of analysts. Worked, as part of a team to, begin analyzing air samples for the MA-DEP Air Phase Petroleum Hydrocarbons method. This included reporting software testing, working on instituting the SOP, IDOCs, canister certifications, and for DOD projects, MDL and LOD studies. Show less
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ANALYTICAL CHEMIST
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Feb 2009 - Nov 2009
(9 month contract) RESPONSIBILITIES Analysis of final radio-pharmaceutical drug product using GC and HPLC techniques. Analysis of incoming drug components to verify specifications following USP methods. GC method development and optimization. ACCOMPLISHMENTS Developed a method for trace solvent analysis using headspace GC Adapted existing resources to USP testing of incoming chemicals using creative solutions. (9 month contract) RESPONSIBILITIES Analysis of final radio-pharmaceutical drug product using GC and HPLC techniques. Analysis of incoming drug components to verify specifications following USP methods. GC method development and optimization. ACCOMPLISHMENTS Developed a method for trace solvent analysis using headspace GC Adapted existing resources to USP testing of incoming chemicals using creative solutions.
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RESEARCH ASSISTANT III
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Nov 2007 - Oct 2008
DOSE ANALYSIS DEPARTMENT DOSE ANALYSIS DEPARTMENT
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ECCS Nationwide Mobile Laboratories
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United States
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Environmental Services
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1 - 100 Employee
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SENIOR CHEMIST
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Aug 2005 - Oct 2007
RESPONSIBILITIES Routine analysis of semi-volatiles and volatiles using GC/MS. GC, and HPLC in fixed based and mobile laboratories. Method development for GC and HPLC analysis. Write SOPs for both field portable and fixed based lab analyses. Convert published methodologies to field portable analyses by reducing preparation steps and analysis times. Client relations and customer service when operating as lead chemist in field. Tracking and reporting analytical results using a variety of analytical techniques, directly to client in field. Manage sample flow and analytical results while working in multi-analyst field jobs. ACCOMPLISHMENTS Developed a field portable/fixed based testing procedure for explosives and propellants by HPLC Developed a viable field portable screening procedure for propellants and nitroaromatics. Show less
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Idaho National Laboratory
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United States
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Research Services
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700 & Above Employee
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(AMWTP) CHEMIST, SYSTEM ADMIN
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Sep 2004 - Aug 2005
MAINTAIN AND TROUBLE SHOOTING OF HGAS SAMPLER AND GC/MS SYSTEM. WROTE CUSTOM SOFTWARE USING THE AGILENT CHEMSTATION MACRO LANGUAGE AS PER CUSTOMER REQUESTS MAINTAIN AND TROUBLE SHOOTING OF HGAS SAMPLER AND GC/MS SYSTEM. WROTE CUSTOM SOFTWARE USING THE AGILENT CHEMSTATION MACRO LANGUAGE AS PER CUSTOMER REQUESTS
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Technical Staff Member
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1999 - 2005
RESPONSIBILITIES Sample and analyze mixed waste (drum headspace) for volatiles by GC/MS prior to shipment to Waste Isolation Pilot Plant (WIPP). Data analysis and batch data report generation for WIPP characterization. Training of personnel from other DOE sites on operation of Headspace Gas Sampling Manifold (HGAS), and all associated software packages. Software QA process on new versions of proprietary HGAS system software. Design Excel spreadsheet templates for automated summary data reports. 24 hour phone and online support of instruments deployed at Rocky Flats Environmental Technology Site.ACCOMPLISHMENTS Attained a DOE “Q” clearance (Top Secret equivalent). Participated in design and implementation of second generation GC/MS HGAS system, including software and mechanical design phases, as well as testing and installation. Designed and carried out sampling plan to determine hydrogen levels in a uranium criticality reactor. Designing and carried out sampling plan to determine hydrogen levels in drums containing depleted uranium waste. Wrote a major revision of a detailed technical procedure for HGAS sampling. Became a subject matter expert for DOE Carlsbad Area Office, for HGAS analysis. Received a distinguished performance award (2001) for contributions to HGAS development team. Show less
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chemist
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1999 - 2004
RESPONSIBILITIES Sample and analyze mixed waste (drum headspace) for volatiles by GC/MS prior to shipment to Waste Isolation Pilot Plant (WIPP). Data analysis and batch data report generation for WIPP characterization. Training of personnel from other DOE sites on operation of Headspace Gas Sampling Manifold (HGAS), and all associated software packages. Software QA process on new versions of proprietary HGAS system software. Design Excel spreadsheet templates for automated summary data reports. 24 hour phone and online support of instruments deployed at Rocky Flats Environmental Technology Site.ACCOMPLISHMENTS Attained a DOE “Q” clearance (Top Secret equivalent). Participated in design and implementation of second generation GC/MS HGAS system, including software and mechanical design phases, as well as testing and installation. Designed and carried out sampling plan to determine hydrogen levels in a uranium criticality reactor. Designing and carried out sampling plan to determine hydrogen levels in drums containing depleted uranium waste. Wrote a major revision of a detailed technical procedure for HGAS sampling. Became a subject matter expert for DOE Carlsbad Area Office, for HGAS analysis. Received a distinguished performance award (2001) for contributions to HGAS development team. Show less
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SENIOR SIENTIST
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Mar 2003 - Sep 2004
OVERSAW MANUFACTURE, TESTING, AND IMPLEMENTATION OF HGAS UNITS. WROTE AND SPECIFIED SOFTWARE REVISIONS FOR WIPP-WAP COMPLIANCE. COMPLETED INSTRUMENT FACTORY ACCEPTANCE TESTING OVERSAW MANUFACTURE, TESTING, AND IMPLEMENTATION OF HGAS UNITS. WROTE AND SPECIFIED SOFTWARE REVISIONS FOR WIPP-WAP COMPLIANCE. COMPLETED INSTRUMENT FACTORY ACCEPTANCE TESTING
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Education
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University of Wisconsin-Green Bay
BS, CHEMISTRY -
University of Wisconsin-River Falls
NA, PRE VET MEDICINE